Journal
ORGANIC LETTERS
Volume 12, Issue 23, Pages 5434-5437Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol102269s
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Asymmetric epoxidation of alpha-substituted acroleins with hydrogen peroxide has been catalyzed by diphenylprolinol diphenylmethylsilyl ether to afford alpha-substituted-beta,beta-unsubstituted-alpha,beta-epoxy aldehyde with excellent enantioselectivity and the generation of a chiral quaternary carbon center. The method was applied to a short synthesis of (R)-methyl palmoxirate.
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