Journal
ORGANIC LETTERS
Volume 12, Issue 19, Pages 4424-4427Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol101931y
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Funding
- National Institutes of Health [CA68682]
- National Science Foundation [0741973]
- WCU (World Class University) [R32-2008-000-10217-0]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [741973] Funding Source: National Science Foundation
- Ministry of Education, Science & Technology (MoST), Republic of Korea [R32-2008-000-10217-0] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Naphthobipyrrole is a potentially useful building block for porphyrin and porphyrin analogue synthesis. Reported here is a simple, generalizable synthetic route to alpha-formylated, beta-substituted naphthobipyrroles and their use in the preparation of binaphthoporphycenes. The resulting binaphthoporphycenes possess a planar geometry as determined via a single-crystal X-ray diffraction analysis; they also display absorption maxima that are bathochromically shifted compared to simple porphycenes.
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