Journal
ORGANIC LETTERS
Volume 12, Issue 11, Pages 2650-2652Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol1008679
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Funding
- National Institutes of Health [GM70483]
- Brigham Young University (Cancer Research Center)
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Two complementary sets of conditions for radical additions of thiols to terminal ynamides are described. The use of 1 equiv of thiol affords the cis-beta-thioenamide adducts in rapid fashion (10 min) and good dr, whereas employing excess thiol and longer reaction times favors the trans products.
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