Journal
ORGANIC LETTERS
Volume 12, Issue 4, Pages 732-735Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol9027978
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Mannich reaction of imines and ketones induced by persistent radical cation salts was investigated, and a series of Mannich bases, beta-aminoketones, were synthesized. A novel cyclization to form the 4-piperidone skeleton was achieved in a tandem process. The reaction can be rationalized as a radical cation process supported by various evidence.
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