Journal
ORGANIC LETTERS
Volume 12, Issue 9, Pages 2004-2007Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol100470g
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Funding
- National Science Foundation [CHE-0742565]
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The concise total synthesis of (-)-aurantioclavine has been achieved by taking advantage of strategies for the asymmetric alkenylation of N-tert-butanesulfinyl imines. The enantiomerically pure natural product was prepared in 6 steps and 27% overall yield by using Rh-catalyzed addition of a N-methyliminodiacetic acid (MIDA) boronate and in 5 steps and 29% yield by employing a Grignard reagent addition sequence.
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