Journal
ORGANIC LETTERS
Volume 12, Issue 20, Pages 4513-4515Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol101887b
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Funding
- North Carolina Biotechnology Center
- National Science Foundation [CHE-0078253]
- Taracept Inc
- NCSU for a North Carolina State University
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A concise synthesis of (S)-macrostomine has been accomplished in five steps from natural nicotine in 19% overall yield via a pyridine Die Is Alder cycloaddition reaction as the key step. A Kumada cross-coupling reaction on a 1-chloroisoquinoline intermediate provided the natural product
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