Journal
ORGANIC LETTERS
Volume 11, Issue 20, Pages 4568-4571Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol9018166
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- The University of Hong Kong
- University Grants Council [AoE 10/01P]
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A variety of secondary benzylic amines; were oxidized to imines in 90% to >99% yields by singlet oxygen generated from oxygen and a porphyrin photosensitizer. On the basis of these reactions, a protocol was developed for oxidative Ugi-type reactions with singlet oxygen as the oxidant. This protocol has been used to synthesize C1(-) and N-functionalized benzylic amines in up to 96% yields.
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