Journal
ORGANIC LETTERS
Volume 11, Issue 4, Pages 1027-1029Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol802974b
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Funding
- National Natural Science Foundation of China [20872131]
- Natural Science Foundation of Zhejiang Province [Y407250]
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Mediated by copper/diethyl azodicarboxylate, regioselective alkynylation of unactivated aliphatic tertiary methylamine with terminal alkyne was successfully established. It is not necessary for the tertiary methylamines to be aryl substituted to modulate the properties of amines. The alkynylation reaction described here has the advantage of simple operation, mild reaction conditions, good to excellent yields, and no need to exclude air and moisture.
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