Journal
ORGANIC LETTERS
Volume 11, Issue 9, Pages 1967-1970Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol9004189
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Funding
- NIH [RO1 CA122256, RO1 A1039987]
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Hemi-phorboxazole A, a minor truncated analogue of phorboxazole A from the marine sponge Phorbas sp., was isolated in a total yield of 16.5 mu g (28 nmol). The structure was elucidated by application of integrated nanomole-scale natural product techniques, including cryomicroprobe NMR, H-1-coupled HSQC, and circular dichroism (CD).
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