Journal
ORGANIC LETTERS
Volume 11, Issue 11, Pages 2385-2388Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol900451d
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Funding
- National Natural Science Foundation of China [20621061, 20772117]
- National Basic Research Program of China [2006CB922003]
- Knowledge Innovation Project of the Chinese Academy of Sciences [KJCX2.YW.H16]
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An efficient methodology for the oxidative addition reaction of various aldehydes with 5,5-dimethylcyclohexane-1,3-dione and 1,3-indandione to selectively afford spiro dihydrofuran and cyclopropane derivatives, promoted by molecular iodine and dimethylaminopyridine under mechanical milling conditions, has been demonstrated. The products were obtained in good to excellent yields. A possible mechanism of this unusual reaction process is proposed.
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