Journal
ORGANIC LETTERS
Volume 11, Issue 7, Pages 1539-1542Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol900194v
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Funding
- British Columbia
- Canada Research Chair Program
- NSERC
- CIHR
- CFI
- MerckFrosst Canada
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Iodobenzene diacetate in MeOH containing a catalytic amount of TFA efficiently oxidizes aldoximes to nitrile oxides. The latter may be trapped in situ with olefins in a bimolecular or an intramolecular mode. The new method enables the execution of tandem oxidative dearomatization of phenols/intramolecular nitrile oxide cycloaddition sequences leading to useful synthetic intermediates.
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