Journal
ORGANIC LETTERS
Volume 11, Issue 7, Pages 1543-1546Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol900131q
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Funding
- NCI [T32CA09112]
- DFG awards [WE 3549/2-1]
- National Institutes of Health [GM 1S10RR13886-01]
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Palladium-catalyzed alpha-arylation and vinylation of dioxolane (S,S)-I, easily obtained from (S)-mandelic acid, proceeds with high yields and excellent diastereoselectivity at room temperature employing commercially available P(t-Bu)(3)center dot HBF4 and Pd(OAc)(2) as a catalytic precursor system. This method displays general utility for a large variety of aryl, heteroaryl, and vinyl bromides.
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