Journal
ORGANIC LETTERS
Volume 10, Issue 11, Pages 2207-2210Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol800619c
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Funding
- NIGMS NIH HHS [R37 GM046059, GM46059, R37 GM046059-16, R01 GM046059] Funding Source: Medline
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The ortho arylation of anilides to form biphenyls via a twofold C-H functionalization/C-C bond-forming process is described. The oxidative coupling takes place in the presence of 5-10 mol % of Pd(OAC)(2), 10-20 mol % of DMSO, and 4-11 equiv of the aryl substrate in TFA under an oxygen atmosphere. No metal-containing cocatalyst is required.
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