Journal
ORGANIC LETTERS
Volume 10, Issue 20, Pages 4577-4579Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol801859c
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Funding
- NSF [CHE 0749916, MRI 0079750, CHE 0091975]
- NIH [RR01654401]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0749916] Funding Source: National Science Foundation
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Re2O7 in CH3CN is a remarkably efficient and mild catalyst for the peroxyacetalization of ketones, aldehydes, or acetals by H2O2 to generate 1,1-dihydroperoxides. Me3SiOReO3 and methyl rhenium trioxide (MTO) are also effective catalysts under these reaction conditions.
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