Journal
ORGANIC LETTERS
Volume 10, Issue 8, Pages 1621-1624Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol8002833
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A novel organocatalyst was developed that effectively catalyzed the reactions of unprotected or protected dihydroxyacetone with a variety of aldehydes to provide syn-aldol products with good yields and ee values up to >99%. Significantly, this amide catalyst was effective with a variety of nonaromatic aldehyde acceptors that had proven difficult in the presence of other catalysts. Reactions of protected dihydroxyacetone proceeded in aqueous media without addition of organic solvents.
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