Journal
ORGANIC LETTERS
Volume 10, Issue 3, Pages 505-507Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol7028788
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A new synthesis of enamides from ketones is disclosed that involves a phosphine-mediated reductive acylation of oximes. The resulting enamides are isolated in good yields (up to 89%) and excellent purity, permitting a subsequent hydrogenation to access enantiopure acetamides at catalyst loadings practical for large-scale applications.
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