Journal
ORGANIC LETTERS
Volume 10, Issue 1, Pages 137-140Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol702729u
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In a synthetic approach to the completely protected C-1-C-12 fragment of the macrocyclic cytotoxic agent tedanolide 1, we carried out the tin-catalyzed Mukaiyama aldol reaction between the 2,3-dialkoxypropanal 5 and the silyl enol ether 6 derived from the ketone 7, which gave, unexpectedly, the anti aldol isomer, rather than the expected syn isomer 4, as the major diastereomer formed.
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