Journal
ORGANIC LETTERS
Volume 10, Issue 5, Pages 909-911Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol703039v
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Funding
- NIGMS NIH HHS [GM-35982, R01 GM035982-19, R01 GM035982] Funding Source: Medline
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C-13 INEPT Diffusion-ordered NMR spectroscopy (DOSY) with an internal reference system was developed to study the aggregation state of THF-solvated LDA dimeric complex. Six components are clearly identified in the diffusion dimension, and their DOSY-generated 13C INEPT spectrum slices agree extremely well with their respective INEPT spectra. The correlation between log D and log FW of the linear least squares fit to reference points of all components is exceptionally high: (r = 0.9985).
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