Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 12, Issue 39, Pages 7678-7681Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ob01369g
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Funding
- National Natural Science Foundation of China [21302109, 21302110, 21375075]
- Taishan Scholar Foundation of Shandong Province
- Excellent Middle-Aged and Young Scientist Award Foundation of Shandong Province [BS2013YY019]
- Scientific Research Foundation of Qufu Normal University [BSQD 2012020]
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A novel iron-catalyzed direct difunctionalization of alkenes with sulfinic acids and dioxygen for the synthesis of beta-ketosulfones has been developed under mild conditions. The present protocol, which utilizes an inexpensive iron salt as the catalyst, readily available benzenesulfinic acids as the sulfonylating reagents, and dioxygen as the oxidant and oxygen source, provides a cost-effective and environmentally benign approach to access various beta-ketosulfones.
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