Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 11, Issue 30, Pages 5042-5046Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ob40767e
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Funding
- Ministero dell'Istruzione, dell'Universita e della Ricerca (MIUR)
- Universita degli Studi di Perugia
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An efficient protocol for the hydrophosphonylation of aromatic and aliphatic aldehydes catalyzed by PS-BEMP under solvent-free conditions (SolFC) has been reported. Addition reactions were performed by using equimolar amounts of reagents and the resulting alpha-hydroxyphosphonates were isolated with simple workup procedures. A large scale protocol for the preparation of a representative alpha-hydroxyphosphonate 3a has been also set up using a flow reactor.
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