Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 11, Issue 20, Pages 3277-3281Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ob40142a
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The dba-free Heck-Matsuda reaction was investigated via direct ESI-MS(/MS) monitoring. Palladium species involved in the reduction of Pd(II) during a Wacker type reaction and several dba-free arylpalladium transient complexes were detected and characterized. Based on these findings, a more comprehensible catalytic cycle for this pivotal reaction is suggested.
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