Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 10, Issue 30, Pages 5774-5779Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ob25407g
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Funding
- Engineering and Physical Sciences Research Council [EP/F069685/1] Funding Source: researchfish
- EPSRC [EP/F069685/1] Funding Source: UKRI
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Using a simple and accessible Teflon AF-2400 based tube-in-tube reactor, a series of pyrroles were synthesised in flow using the Paal-Knorr reaction of 1,4-diketones with gaseous ammonia. An inline flow titration technique allowed measurement of the ammonia concentration and its relationship to residence time and temperature.
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