Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 10, Issue 39, Pages 7869-7871Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ob26430g
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Funding
- National Basic Research Program of China [2012CB822100]
- National Natural Science Foundation of China (NSFC) [21072017, 21072016, 20972012]
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We have developed a new KI-catalyzed method for the imidation of an sp(3) C-H bond adjacent to an amide nitrogen atom by using TBHP (tert-butyl hydroperoxide, 70% aqueous solution) as the oxidant. This novel procedure tolerated air and moisture and provided a series of novel products in moderate to excellent yields under mild conditions.
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