Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 10, Issue 39, Pages 7863-7868Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ob26423d
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- National Overseas Scholarship from the Indian Ministry of Social Justice and Empowerment [GF6-352746]
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Substituted pyrrolines are available by ring closure initiated by direct nucleophilic attack of stabilized enolates at the nitrogen of oximes activated with a leaving group, in a process which effectively out-competes the more usual Beckmann rearrangement. Subsequent reduction provides diastereoselective access to the corresponding pyrrolidines. This provides a rapid route to saturated heterocyclic systems from readily available precursors.
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