Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 10, Issue 17, Pages 3531-3537Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ob07074j
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Funding
- Irish Research Council for Science, Engineering and Technology (IRCSET)
- Science Foundation Ireland (SFI) [08/RFP/CHE1251, 09/IN.1/B2627]
- Science Foundation Ireland (SFI) [08/RFP/CHE1251] Funding Source: Science Foundation Ireland (SFI)
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A mild method for the facile removal of phosphine oxide from the crude products of Wittig and Appel reactions is described. Work-up with oxalyl chloride to generate insoluble chlorophosphonium salt (CPS) yields phosphorus-free products for a wide variety of these reactions. The CPS product can be further converted into phosphine.
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