Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 6, Pages 1938-1947Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ob00815j
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Funding
- Paul Mellon Fellowship
- EPSRC
- Royal Society
- BP [1702]
- EPSRC [EP/F069685/1, EP/G028125/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/F069685/1, EP/G028125/1] Funding Source: researchfish
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Having demonstrated in the preceding publication the flow synthesis of aryl azides, we describe here a general protocol for the in-line purification of these versatile intermediates. As part of this investigation, we evaluated the use of ReactIR 45m as a tool for real-time detection of hazardous azide contaminants. This azide synthesis and purification process was then incorporated into a multistep flow sequence to generate a small collection of 5-amino-4-cyano-1,2,3-triazoles directly from aniline starting materials in a fully automated fashion.
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