Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 6, Pages 1927-1937Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0ob00813c
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Funding
- Paul Mellon Fellowship
- Syngenta
- EPSRC
- Royal Society
- BP [1702]
- EPSRC [EP/F069685/1, EP/G028125/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/F069685/1, EP/G028125/1] Funding Source: researchfish
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Here we describe general flow processes for the synthesis of alkyl and aryl azides, and the development of a new monolithic triphenylphosphine reagent, which provides a convenient format for the use of this versatile reagent in flow. The utility of these new tools was demonstrated by their application to a flow Staudinger aza-Wittig reaction sequence. Finally, a multistep aza-Wittig, reduction and purification flow process was designed, allowing access to amine products in an automated fashion.
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