Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 9, Pages 3122-3125Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ob05167a
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Funding
- University of Cyprus, the Cyprus Research Promotion Foundation [YFEIA/BIOSigma/0308(BIE)/13]
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Stille and Suzuki-Miyaura reactions of 7-iodo-1,3-diphenyl-1,4- dihydro-1,2,4-benzotriazin-4-yl are presented as rare examples of cross-coupling reactions with stable organic radicals. Both the Stille and Suzuki-Miyaura reactions are in most cases high yielding but the latter are cleaner while the former are faster and are accompanied by 1,3-diphenyl-1,2,4-benzotriazin- 7(H)-one as by-product. A range of 7-aryl and 7-heteroaryl-1,2,4-benzotriazinyls have been synthesized and characterized using standard spectroscopic and spectrometric means.
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