Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 9, Issue 16, Pages 5630-5632Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1ob05335c
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- Council of Scientific and Industrial Research (CSIR), New Delhi, India
- Council of Scientific and Industrial Research (CSIR), New Delhi [P-81-113]
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A convergent synthesis of the macrolactone core of amphidinolactone A has been achieved, in a 10 step linear sequence with 32% overall yield, through a ring-closing metathesis reaction as the macrolactonization step. The RCM precursor was obtained by the union of acid and alcohol fragments derived from (R)-epichlorohydrin and (R)-2,3-O-isopropylidene glyceraldehyde, respectively.
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