Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 7, Issue 13, Pages 2788-2795Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b901911a
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A highly practical route to oligostilbenoid natural products is described. A regioselective Bi(OTf)(3)-catalyzed cyclodehydration provided ready access to 3-arylbenzofuran. Pd-catalyzed direct C-H activation of benzofuran and subsequent cross-coupling with aryl halide was successfully implemented for the introduction of aryl group at the C2 position of benzofuran. Further manipulation of the 2,3-diarylbenzofuran led to the efficient total synthesis of permethylated analogues of viniferifuran, malibatol A, and shoreaphenol.
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