Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 7, Issue 12, Pages 2635-2644Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b822989a
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- MUR-Italy
- Italian National Research Council (CNR)
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An approach to the synthesis of pseudo-oligosaccharides based on the cross-metathesis reaction between distinct sugar-olefins, followed by intramolecular cyclization of the obtained heterodimer, is presented. In particular, the relative efficiency of two alternative approaches, the straightforward cross-metathesis reaction and the two-step procedure (self-metathesis followed by cross-metathesis), was explored and compared for diverse sugar-olefin substrates. Some representative examples of intramolecular cyclization using iodine as an electrophilic promoter, are also reported.
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