Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 7, Issue 19, Pages 3910-3913Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b912686d
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We present the first synthesis of calix[4] arene-based S-glycoclusters via photoinduced multiple thiol-ene coupling of tetra-and octa-allyl calix[4]arenes with peracetylated glucosyl thiol (67-88% yields). Moreover we describe the dual clustering at the upper and lower rim of a calix[4] arene with two different sugars (galactose and glucose) via sequential copper(I)-catalyzed azide-alkyne cycloaddition and photoinduced thiol-ene coupling.
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