Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 6, Issue 15, Pages 2686-2691Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b803451f
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Funding
- NATIONAL INSTITUTE OF GENERAL MEDICAL SCIENCES [R41GM075436] Funding Source: NIH RePORTER
- NIGMS NIH HHS [1 R41 GM 075436-01] Funding Source: Medline
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We report herein the first synthesis of linear and branched mannose oligosaccharides using fluorous-tag assistance with reagents and FSPE protocols that are amenable to automation. The particular fluorous linker proved to maintain solubility of the growing oligosaccharide chain such that identical reaction solvent conditions and purification protocols could be used between glycosylation and deprotection reactions, thereby rendering the procedures amenable to automation.
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