4.2 Article

Annealing of PrF3 nanoparticles by microwave irradiation

Journal

OPTICS AND SPECTROSCOPY
Volume 116, Issue 5, Pages 721-723

Publisher

PLEIADES PUBLISHING INC
DOI: 10.1134/S0030400X14050026

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Funding

  1. Russian Foundation for Basic Research [14-02-31361 mol_a]
  2. Ministry of Education and Science of the Russian Federation [02.G25.31.0029]

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The influence of microwave irradiation on the recovery of nanocrystalline PrF3 powders has been experimentally analyzed by nuclear magnetic resonance (NMR) at T = 1.5 K. It is established that the relaxation times of Pr-141 and F-19 nuclei rise significantly with an increase in the hydrothermal-treatment time, whereas the Pr-141 NMR spectra narrow, which indicates a decrease in the number of defects in the lattices of nanosamples.

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