Journal
TETRAHEDRON LETTERS
Volume 56, Issue 31, Pages 4569-4573Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.06.024
Keywords
Copper-catalyzed; Esterification; Formyl; TBHP; Salicylaldehyde
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Funding
- National Science & Technology Major Project 'Key New Drug Creation and Manufacturing Program', China [2009ZX09301-001]
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A copper-catalyzed oxidative esterification of ortho-formyl phenols with aldehydes using TBHP as oxidant in water is developed. Besides aromatic and aliphatic aldehydes, benzylic alcohols are also suitable for this reaction. The sensitive formyl group remains intact under oxidative conditions. This method provides an alternative protocol for classical esterification reactions. (C) 2015 Elsevier Ltd. All rights reserved.
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