Journal
TETRAHEDRON LETTERS
Volume 56, Issue 19, Pages 2472-2475Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.03.102
Keywords
Huisgen-click reaction; Supercritical carbon dioxide; Cycloaddition; Triazoles
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Funding
- Natural Science Foundation of China [21172058]
- Scientific Research Foundation for Doctors [01036500508]
- Youth Foundation of Henan Normal University [2012QK11]
- Foundation of Henan Scientific and Technological Committee [132300410167]
- Foundation of He'nan Educational Committee [14A350005]
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An efficient protocol for Huisgen-click reaction catalyzed by Cu(OAc)(2)center dot H2O for the synthesis of 1, 4-disubstituted triazoles has been developed in supercritical carbon dioxide (scCO(2)) in the absence of ligand at 36 degrees C. The protocol could afford the corresponding products in excellent yield at very low catalyst loadings (0.01 mol %). (C) 2015 Elsevier Ltd. All rights reserved.
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