Journal
TETRAHEDRON LETTERS
Volume 56, Issue 26, Pages 3999-4001Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2015.04.037
Keywords
Fellutamide; Neurodegenerative diseases; Tuberculosis proteasome; Solution phase synthesis; Peptide coupling
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Funding
- CSIR [ORIGIN: CSC-0108]
- J.C. Bose & CSIR Bhatnagar Fellowship
- CNRS (University of Rennes I)
- CEFIPRA/IFCPAR
- CSIR, New Delhi
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A convenient solution phase approach for the synthesis of fellutamide B with efficient purification techniques has been demonstrated on the molecule for the first time. The strategy involves the use of natural amino acids as starting materials and classical peptide coupling reactions. The synthesis has been achieved in 10 steps with overall yield of 26.7% making the synthesis facile. (C) 2015 Elsevier Ltd. All rights reserved.
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