Journal
SYNTHETIC COMMUNICATIONS
Volume 45, Issue 18, Pages 2122-2129Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2015.1066391
Keywords
Alkynes; cyclization; ligand; nitroxides; Sonogashira coupling
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Funding
- Hungarian National Research Fund [OTKA K81123, K104956]
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3-Substituted and 3,4-disubstituted pyrroline nitroxides containing an ethynyl group or two ethynyl groups were achieved by the reaction of a paramagnetic aldehydes with dimethyl (1-diazo-2-oxopropyl)phosphonate (Bestmann-Ohira reagent). The new compounds containing an ethynyl group were found to be useful building blocks in Sonogashira coupling, cyclization, and cycloaddition reactions producing potentially azido-specific cross-linking spin labels, paramagnetic ligands, and polyradical scaffolds.
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