Journal
SYNTHESIS-STUTTGART
Volume 48, Issue 1, Pages 85-96Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0035-1560481
Keywords
isoselenocyanates; isocyanides; selenium; phase-transfer catalysis
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Funding
- National Science Centre, Poland [N N209 044739]
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Isoselenocyanates were synthesized by two methods under phase-transfer conditions (50% aq NaOH, CH2Cl2, Aliquat 336); the first started from isocyanides and selenium and gave isoselenocyanates in 61-89% yields, while the second started from amines and used chloroform and selenium, by applying sequentially the Hofmann isonitrile synthesis and the addition of selenium, in 4-70% yields.
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