Journal
SYNLETT
Volume 26, Issue 18, Pages 2557-2560Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0035-1560180
Keywords
C(sp(3))-H/C(sp(2))-H cross-dehydrogenative coupling; ethers; enamides; beta-oxo ketones; radicals
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Funding
- National Natural Science Foundation of China [21102130]
- Natural Science Foundation of Zhejiang Province [LY14B020005]
- 863 Program [2013AA065005]
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A new MnO2-catalyzed oxidative alkylation of enamides with a C(sp(3))-H bond adjacent to an oxygen atom is described. This method achieves a C(sp(3))-H/C(sp(2))-H cross-dehydrogenative coupling and hydrolysis, thus providing efficient and general access to a variety of beta-oxo ketones.
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