Journal
SYNLETT
Volume 27, Issue 3, Pages 369-374Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0035-1560594
Keywords
ambrox; natural products; titanocene; radical chemistry; diastereoselective synthesis
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Funding
- Spanish MICINN [CTQ2008-06790, CTQ2010-17115, CTQ2011-24443]
- Regional Government of Andalucia [P07-FQM-3213, P10-FQM-6050]
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A synthesis of (+/-)-ambrox, a compound with delicious ambergris-type scent, is presented. The key step is a highly diastereoselective titanocene(III)-catalyzed radical tandem cyclization of a farnesol derivative.
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