CdTe detector use for PIXE characterization of TbCoFe thin films

Peltier cooled CdTe detectors have good efficiency beyond the range of energies normally covered by Si(Li) detectors, the most common detectors in PIXE applications. An important advantage of CdTe detectors is the possibility of studying K X-rays lines instead the L X-rays lines in various cases since CdTe detectors present an energy efficiency plateau reaching 70 keV or more. The ITN CdTe useful energy range starts at K-K-alpha (3.312 key) and goes up to 120 keV, just above the energy of the lowest gamma-ray of the F-19(p, p'gamma)F-19 reaction. In the new ITN HRHE-PIXE line, a CdTe detector is associated to a POLARIS microcalorimeter X-ray detector built by Vericold Technologies GmbH (an Oxford Instruments Group Company). The ITN POLARIS has a resolution of 15 eV at 1.486 keV (Al-K-alpha) and 24 eV at 10.550 key (Pb-L-alpha 1). In the present work, a TbCoFe thin film deposited on a Si substrate was analysed at the HRHE-PIXE system. The good efficiency of the CdTe detector at 45 keV (Tb-K-alpha), and the excellent resolution of POLARIS microcalorimeter at 6.403 keV (Fe-K-alpha), are presented and the new possibilities open to the IBA analysis of systems with traditionally overlapping X-rays and near mass elements are discussed. (C) 2010 Elsevier B.V. All rights reserved.