Journal
NEW JOURNAL OF CHEMISTRY
Volume 38, Issue 11, Pages 5626-5632Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4nj01329h
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Funding
- Basic Science Research Program through the National Research Foundation of Korea (NRF) - Ministry of Science, ICT & Future Planning [2013R1A1A1A05006634]
- Research and Development Program of the Korea Institute of Energy Research (KIER) [B4-2432-03]
- National Research Foundation of Korea [2013R1A1A1A05006634] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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In the present work, we synthesized magnetically separable Pd/Fe3O4/charcoal nanocatalysts by simple solid-state grinding of a mixture of salts and the simultaneous thermal decomposition of the salts. The highly loaded Pd nanoparticles (20 wt%) were well dispersed in the porous charcoal, with an average diameter of similar to 5 nm and clean surfaces without any surfactant. Moreover, the simultaneously obtained Fe3O4 nanoparticles (10 wt%) had good superparamagnetic character, enabling quick separation of the catalyst from the products and re-dispersion in the reaction solution. The bifunctional catalyst showed a high product time yield with various substituted aryl halides and aryl boronic acids.
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