Journal
NANOSCALE
Volume 4, Issue 11, Pages 3394-3398Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2nr30612c
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Funding
- Ministry of Education, Culture, Sports and Science for Technology of Japan (MEXT)
- JST
- Nippon Sheet Glass Foundation for Materials Science and Engineering
- [23241025]
- Grants-in-Aid for Scientific Research [23241025] Funding Source: KAKEN
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Described here is how to synthesize one-dimensional ammonium tungsten bronze ((NH4)(x)WO3) by a facile solvothermal approach in which ethylene glycol and acetic acid were employed as solvents and ammonium paratungstate was used as a starting material, as well as how to develop the near infrared absorption properties of (NH4)(x)WO3 nanorods for application as a solar light control filter. The as-obtained product was characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), thermogravimetry (TG), atomic force microscope (AFM) and UV-Vis-NIR spectra. The SEM and TEM images clearly revealed that the obtained sample possessed rod/fiber-like morphologies with diameters around 120 nm. As determined by UV-Vis-NIR optical measurement, the thin film consisted of (NH4)(x)WO3 nanoparticles, which can selectively transmit most visible lights, but strongly absorb the near-infrared (NIR) lights and ultraviolet rays. These interesting optical properties make the (NH4)(x)WO3 nanorods suitable for the solar control windows.
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