Journal
NANOSCALE
Volume 4, Issue 5, Pages 1557-1560Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2nr11690a
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Funding
- Energy Frontier Research Center on Science Based Nano-Structure Design and Synthesis of Heterogeneous Functional Materials for Energy Systems (HeteroFoaM Center)
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-SC0001061, DE-AC02-06CH11357]
- National Science Foundation [CBET-1134052]
- Brookhaven Science Associates, LLC [DE-AC02-98CH10886]
- Div Of Chem, Bioeng, Env, & Transp Sys
- Directorate For Engineering [1134052] Funding Source: National Science Foundation
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Nano-structures of nickel (Ni) and nickel subsulfide (Ni3S2) materials were studied and mapped in 3D with high-resolution x-ray nanotomography combined with full field XANES spectroscopy. This method for characterizing these phases in complex microstructures is an important new analytical imaging technique, applicable to a wide range of nanoscale and mesoscale electrochemical systems.
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