Journal
MONATSHEFTE FUR CHEMIE
Volume 146, Issue 2, Pages 351-356Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-014-1373-8
Keywords
Azo-compounds; Benzeneseleninic acid; Nitrobenzeneseleninic acid; Nitration
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Funding
- Ministry of Education, Culture, Sports, Science and Technology (MEXT) [16002007]
- JSPS
- University of Stavanger
- Research program, Green Production Chemistry
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Hydrogenolysis of 3-nitrobenzeneseleninic acid and 3-bromo-4-nitrobenzeneseleninic acid under standard conditions (Pd/C, H-2 1 atm in MeOH) gave exclusively the corresponding azo-compounds. Nitration of the azo-compounds with HNO3 in H2SO4 at 0 A degrees C yielded solely 3-nitrobenzeneseleninic acid and 3-bromo-4-nitrobenzeneseleninic acid in return.
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