Journal
MONATSHEFTE FUR CHEMIE
Volume 144, Issue 7, Pages 1081-1085Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-012-0920-4
Keywords
IPL576,092; Allylic oxidation; Hydroborations; alpha,beta-unsaturated ketones; Steroids
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Funding
- National Natural Science Foundation of China [20472070]
- State University College of Innovative Experimental Projects [101067319]
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An improved and efficient preparation of IPL576,092 was developed. The synthetic route involves selective allylic oxidation of a dagger(5)-sterols and subsequent hydroboration-oxidation as the key steps. In addition, two analogues were readily synthesized from commercially available steroidal compounds in two steps in the same way.
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