Journal
MONATSHEFTE FUR CHEMIE
Volume 144, Issue 10, Pages 1455-1459Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-013-1036-1
Keywords
IR spectroscopy; Raman spectroscopy; Crystal structure; Coordination chemistry; Fluorides
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Funding
- Slovenian Research Agency (ARRS)
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X-ray crystal structure determination at 200 K revealed that N2H5CdF3 crystallizes in the orthorhombic space group Pnam, with unit cell dimensions a = 1,421.0(2), b = 694.29(11), c = 447.52(7) pm. The structure consists of N2H5 (+) cations and double Cd-F chains interconnected by a hydrogen bonding network. The N-N stretching vibration in N2H5CdF3 is active in infrared and Raman spectroscopy with an N-N stretching infrared band at 1,002 cm(-1) and a Raman band at 1,008 cm(-1).
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