Journal
MONATSHEFTE FUR CHEMIE
Volume 141, Issue 9, Pages 975-978Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-010-0353-x
Keywords
Acetylation; Economical acidic ionic liquid; Catalyst; Acetic anhydride
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Funding
- SRTP of Anhui University of Technology [09016]
- Education Department of Anhui Province, China [KJ2010A339]
- Foundation for Young Talents in the College of Anhui Province, China [2010SQRL033ZD]
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Rapid and efficient acetylation of alcohols and phenols with acetic anhydride is performed in the presence of economical Bronsted acidic ionic liquids that bear a propanesulfonic acid group on a morpholinium cation as catalysts under solvent-free conditions. [MMPPA][HSO4] (N-methylmorpholinium propanesulfonic acid ammonium hydrogensulfate) was proven to be the most active catalyst, and after removal of water, it could be recycled and reused for up to four times without a noticeable decrease in catalytic activity.
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