Journal
MONATSHEFTE FUR CHEMIE
Volume 140, Issue 1, Pages 61-64Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-008-0004-7
Keywords
Saccharin; Saccharin sulfonic acid; Alcohols; Trimethylsilylation; Hexamethyldisilazane
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Funding
- University of Guilan Research Council
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Saccharin sulfonic acid was easily prepared by the reaction of saccharin with neat chlorosulfonic acid at room temperature. This reagent is efficiently able to catalyze the chemoselective trimethylsilylation of alcohols with hexamethyldisilazane in the presence of amines and thiols.
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